Download e-book for kindle: A Primer on Quality in the Analytical Laboratory by John Kenkel

By John Kenkel

Modern-day commercial laboratory analyst encounters concerns comparable to quality controls, caliber insurance ISO 9000, ordinary working approaches, calibration, typical reference fabrics, statistical keep an eye on, regulate charts, talent trying out, validation, procedure suitability, chain of custody, stable laboratory practices, protocol, and audits. In a well-written and readable variety, A Primer on caliber within the Analytical Laboratory presents an creation to caliber, criteria, and rules within the analytical laboratory and serves as a useful source to a myriad of laboratory practices.Features

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Extra resources for A Primer on Quality in the Analytical Laboratory

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Sometimes, in order to better assure the “representative” status, a series of samples are obtained from different parts of the bulk system and then combined into one sample. This kind of sample is called a composite sample. A composite sample is useful in situations in which it is likely that the substance to be determined is not homogeneously distributed throughout the entire system. For example, when determining the fertilizer needs of a person’s lawn, it might be best to obtain a composite sample because the phosphate level (for example) in one part of the lawn might not be the same as in another part.

The viscosity is dependent on temperature, so the measurement must take place with the tube immersed in a constant-temperature bath. Calibration involves measuring this time for a standard substance, such as an oil for which the viscosity and density are known, in order to calculate the calibration constant. It is an example of a calibration for which the response for a standard substance must be established and then correlated with the unknowns. Some viscosity tubes are calibrated at the factory, in which case a certifcate of calibration, giving the calibration constant, is shipped with the tube.

15 A control chart showing a sudden change, a “stair-step” change. This could result from a system component that was replaced, such as a light source in a spectrophotometer, or a recalibration of a component, such as a viscometer tube. 16 A control chart showing sporadic results starting with Day 18. This behavior would indicate the sudden introduction of random error, such as what might occur when a new analyst is assigned to the task. 17 An illustration of signal and noise. Detection limit is defined as the concentration that produces a signal that is double the noise level.

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